BMRB: 15188

backbone and side chain methly order parameters and correlation times for calcium-saturated calmodulin

Authors

Frederick, K.K., Marlow, M.S., Valentine, K.G., Wand, J.

Assembly

calmodulin

Entity

1. calmodulin (polymer, Thiol state: not present), 148 monomers, 16705.23 Da Detail

ADQLTEEQIA EFKEAFSLFD KDGDGTITTK ELGTVMRSLG QNPTEAELQD MINEVDADGN GTIDFPEFLT MMARKMKDTD SEEEIREAFR VFDKDGNGYI SAAELRHVMT NLGEKLTDEQ VDEMIREADI DGDGQVNYEE FVQMMTAK

Formula weight

16705.23 Da

Source organism

Gallus gallus

Exptl. method

solution NMR

Data set

order_parameters

Order parameters

134 S² values in 2 lists
Pressure 1 atm, Temperature 308 K, pH 6.5 Detail

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Pressure 1 atm, Temperature 308 K, pH 6.5

Experiment name 2D 1H-15N HSQC, 2D 1H-13C HSQC

List #1 backbone_order_parameters, Details NMR derived backbone N-H bond vector model-free squared generalized order parameters for calcium-saturated CaM determined at 500 and 600 MHz (1H)

List #2 methyl_order_parameters, Details NMR derived side-chain model-free squared generalized order parameters for the symmetry axis of methyl groups of calcium-saturated CaM determined with relaxation data obtained at 500 and 600 MHz (1H).

Release date

2007-10-04

Citation

Conformational entropy in molecular recognition by proteins
Frederick, K.K., Marlow, M.S., Valentine, K.G., Wand, J.
Nature (2007), 448, 325-329, PubMed 17637663 , DOI 10.1038/nature05959 , Abstract

Related entities 1. calmodulin, : 1 : 117 : 181 entities Detail

Interaction partners 1. calmodulin, : 1 interactors Detail

Experiments performed 4 experiments Detail