Backbone and 13C and 1H assignments for acid unfolded state and urea unfolded state of CTL9
AAEELANAKK LKEQLEKLTV TIPAKAGEGG RLFGSITSKQ IAESLQAQHG LKLDKRKIEL ADAIRALGYT NVPVKLHPEV TATLKVHVTE QK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 61.1 % (656 of 1073) | 51.4 % (288 of 560) | 66.9 % (279 of 417) | 92.7 % (89 of 96) |
Backbone | 97.4 % (532 of 546) | 94.1 % (176 of 187) | 98.9 % (267 of 270) | 100.0 % (89 of 89) |
Sidechain | 34.1 % (209 of 613) | 30.0 % (112 of 373) | 41.6 % (97 of 233) | 0.0 % (0 of 7) |
Aromatic | 0.0 % (0 of 30) | 0.0 % (0 of 15) | 0.0 % (0 of 15) | |
Methyl | 24.6 % (32 of 130) | 24.6 % (16 of 65) | 24.6 % (16 of 65) |
1. CTL9
AAEELANAKK LKEQLEKLTV TIPAKAGEGG RLFGSITSKQ IAESLQAQHG LKLDKRKIEL ADAIRALGYT NVPVKLHPEV TATLKVHVTE QKSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298.2 (±2) K, pH 2.0 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | CTL9 | [U-99% 13C; U-99% 15N] | 1 mM | |
2 | H2O | natural abundance | 90 % | |
3 | D2O | [U-100% 2H] | 10 % |