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13C and 15N Chemical Shift Assignments for the fd Bacteriophage
Authors
Goldbourt, A., Abramov, G., Morag, O.
Assembly
fd bacteriophage
Entity
1. fd bacteriophage (polymer, Thiol state: not available), 50 monomers, 5238.958 Da Detail

AEGDDPAKAA FDSLQASATE YIGYAWAMVV VIVGATIGIK LFKKFTSKAS


Formula weight
5238.958 Da
Source organism
Escherichia coli
Exptl. method
SOLID-STATE NMR
Data set
assigned_chemical_shifts
Chem. Shift Complete
Sequence coverage: 96.0 %, Completeness: 84.8 %, Completeness (bb): 89.7 % Detail

Polymer type: polypeptide(L)

Total13C15N
All84.8 % (234 of 276)86.2 % (194 of 225)78.4 % (40 of 51)
Backbone89.7 % (175 of 195)92.5 % (135 of 146)81.6 % (40 of 49)
Sidechain81.1 % (103 of 127)82.4 % (103 of 125) 0.0 % (0 of 2)
Aromatic65.5 % (19 of 29)67.9 % (19 of 28) 0.0 % (0 of 1)
Methyl81.8 % (27 of 33)81.8 % (27 of 33)

1. fd

AEGDDPAKAA FDSLQASATE YIGYAWAMVV VIVGATIGIK LFKKFTSKAS

Sample

Solvent system TRIS BUFFER PH8, Temperature 273 K, pH 8 (±0.1)


#NameIsotope labelingTypeConcentration
1fd[U-99% 13C; U-99% 15N]7.0 ~ 15.0 mg
2Trisnatural abundance

Release date
2011-06-22
Citation
Magic-angle spinning NMR of a class I filamentous bacteriophage virus
Abramov, G., Morag, O., Goldbourt, A.
J. Phys. Chem. B (2011), 115, 9671-9680, PubMed 21702439 , DOI 10.1021/jp2040955 ,
Related entities 1. fd bacteriophage, : 1 : 7 : 4 : 4 : 9 entities Detail
Experiments performed 4 experiments Detail