CR1~1-2
EAEAAGQCNA PEWLPFARPT QLTDEFEFPI GTYLNYECRP GYSGRPFSII CLKNSVWTGA KDRCRRKSCR NPPDPVNGMV HVIKGIQFGS QIKYSCTKGY RLIGSSSATC IISGDTVIWD QETPICDR
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 87.9 % (1294 of 1472) | 83.4 % (642 of 770) | 92.6 % (529 of 571) | 93.9 % (123 of 131) |
Backbone | 96.0 % (718 of 748) | 96.1 % (247 of 257) | 95.4 % (356 of 373) | 97.5 % (115 of 118) |
Sidechain | 81.9 % (689 of 841) | 77.0 % (395 of 513) | 90.8 % (286 of 315) | 61.5 % (8 of 13) |
Aromatic | 89.2 % (116 of 130) | 89.2 % (58 of 65) | 88.7 % (55 of 62) | 100.0 % (3 of 3) |
Methyl | 93.9 % (107 of 114) | 93.0 % (53 of 57) | 94.7 % (54 of 57) |
1. CR1 1-2
EAEAAGQCNA PEWLPFARPT QLTDEFEFPI GTYLNYECRP GYSGRPFSII CLKNSVWTGA KDRCRRKSCR NPPDPVNGMV HVIKGIQFGS QIKYSCTKGY RLIGSSSATC IISGDTVIWD QETPICDRSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 310 K, pH 4
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | CR1 1-2 | [U-99% 13C; U-99% 15N] | 0.56 mM | |
2 | sodium acetate | [U-100% 2H] | 20 mM | |
3 | H2O | natural abundance | 90 % | |
4 | D2O | natural abundance | 10 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 310 K, pH 4
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | CR1 1-2 | [U-99% 13C; U-99% 15N] | 0.56 mM | |
6 | sodium acetate | [U-100% 2H] | 20 mM | |
7 | D2O | natural abundance | 100 % |