1H, 15N, 13C Chemical Shifts of Recombinant Rat Ferrocytochrome b5, A conformation
DKDVKYYTLE EIQKHKDSKS TWVILHHKVY DLTKFLEEHP GGEEVLREQA GGDATENFED VGHSTDAREL SKTYIIGELH PDDRSKIAKP SETL
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 76.9 % (844 of 1098) | 76.9 % (440 of 572) | 72.9 % (314 of 431) | 94.7 % (90 of 95) |
Backbone | 94.8 % (529 of 558) | 97.4 % (186 of 191) | 91.7 % (253 of 276) | 98.9 % (90 of 91) |
Sidechain | 62.1 % (390 of 628) | 66.7 % (254 of 381) | 56.0 % (136 of 243) | 0.0 % (0 of 4) |
Aromatic | 14.8 % (13 of 88) | 25.0 % (11 of 44) | 4.7 % (2 of 43) | 0.0 % (0 of 1) |
Methyl | 83.0 % (78 of 94) | 89.4 % (42 of 47) | 76.6 % (36 of 47) |
1. cytochrome b5
DKDVKYYTLE EIQKHKDSKS TWVILHHKVY DLTKFLEEHP GGEEVLREQA GGDATENFED VGHSTDAREL SKTYIIGELH PDDRSKIAKP SETLTemperature 313 (±1) K, pH 7.0 (±0.2), Details 4mM 15N, 13C labeled in 100 mM phosphate pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | cytochrome b5 | [U-15N; U-13C] | 4 mM | |
2 | phosphate | 100 mM |