Backbone NMR Assignments of a High Molecular Weight Protein (47kD), Cyclic AMP Receptor Protein (apo-CRP)
VLGKPQTDPT LEWFLSHCHI HKYPSKSTLI HQGEKAETLY YIVKGSVAVL IKDEEGKEMI LSYLNQGDFI GELGLFEEGQ ERSAWVRAKT ACEVAEISYK KFRQLIQVNP DILMRLSAQM ARRLQVTSEK VGNLAFLDVT GRIAQTLLNL AKQPDAMTHP DGMQIKITRQ EIGQIVGCSR ETVGRILKML EDQNLISAHG KTIVVYGTR
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 44.4 % (1099 of 2475) | 23.3 % (300 of 1290) | 62.9 % (604 of 961) | 87.1 % (195 of 224) |
Backbone | 80.5 % (1000 of 1242) | 51.6 % (221 of 428) | 95.7 % (585 of 611) | 95.6 % (194 of 203) |
Sidechain | 20.2 % (288 of 1426) | 9.3 % (80 of 862) | 38.1 % (207 of 543) | 4.8 % (1 of 21) |
Aromatic | 0.0 % (0 of 146) | 0.0 % (0 of 73) | 0.0 % (0 of 71) | 0.0 % (0 of 2) |
Methyl | 15.2 % (40 of 264) | 12.9 % (17 of 132) | 17.4 % (23 of 132) |
1. Cyclic AMP Receptor Protein
VLGKPQTDPT LEWFLSHCHI HKYPSKSTLI HQGEKAETLY YIVKGSVAVL IKDEEGKEMI LSYLNQGDFI GELGLFEEGQ ERSAWVRAKT ACEVAEISYK KFRQLIQVNP DILMRLSAQM ARRLQVTSEK VGNLAFLDVT GRIAQTLLNL AKQPDAMTHP DGMQIKITRQ EIGQIVGCSR ETVGRILKML EDQNLISAHG KTIVVYGTRTemperature 313 (±0.5) K
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Cyclic AMP Receptor Protein | [U-90% 2H; U-95% 13C; U-95% 15N] | 0.6 mM |