Backbone 1H,13C and 15N chemical shift assignment for the maltotriose-bound state of 2H,13C,15N-labeled maltodextrin-binding protein
KTEEGKLVIW INGDKGYNGL AEVGKKFEKD TGIKVTVEHP DKLEEKFPQV AATGDGPDII FWAHDRFGGY AQSGLLAEIT PDKAFQDKLY PFTWDAVRYN GKLIAYPIAV EALSLIYNKD LLPNPPKTWE EIPALDKELK AKGKSALMFN LQEPYFTWPL IAADGGYAFK YENGKYDIKD VGVDNAGAKA GLTFLVDLIK NKHMNADTDY SIAEAAFNKG ETAMTINGPW AWSNIDTSKV NYGVTVLPTF KGQPSKPFVG VLSAGINAAS PNKELAKEFL ENYLLTDEGL EAVNKDKPLG AVALKSYEEE LAKDPRIAAT MENAQKGEIM PNIPQMSAFW YAVRTAVINA ASGRQTVDEA LKDAQTRITK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 47.3 % (2042 of 4316) | 26.6 % (596 of 2237) | 65.2 % (1104 of 1692) | 88.4 % (342 of 387) |
Backbone | 82.2 % (1791 of 2178) | 54.4 % (407 of 748) | 96.6 % (1044 of 1081) | 97.4 % (340 of 349) |
Sidechain | 23.8 % (589 of 2479) | 12.8 % (190 of 1489) | 41.7 % (397 of 952) | 5.3 % (2 of 38) |
Aromatic | 2.4 % (9 of 378) | 3.7 % (7 of 189) | 1.1 % (2 of 181) | 0.0 % (0 of 8) |
Methyl | 28.2 % (118 of 418) | 21.1 % (44 of 209) | 35.4 % (74 of 209) |
1. maltodextrin-binding protein
KTEEGKLVIW INGDKGYNGL AEVGKKFEKD TGIKVTVEHP DKLEEKFPQV AATGDGPDII FWAHDRFGGY AQSGLLAEIT PDKAFQDKLY PFTWDAVRYN GKLIAYPIAV EALSLIYNKD LLPNPPKTWE EIPALDKELK AKGKSALMFN LQEPYFTWPL IAADGGYAFK YENGKYDIKD VGVDNAGAKA GLTFLVDLIK NKHMNADTDY SIAEAAFNKG ETAMTINGPW AWSNIDTSKV NYGVTVLPTF KGQPSKPFVG VLSAGINAAS PNKELAKEFL ENYLLTDEGL EAVNKDKPLG AVALKSYEEE LAKDPRIAAT MENAQKGEIM PNIPQMSAFW YAVRTAVINA ASGRQTVDEA LKDAQTRITKTemperature 310 (±0.5) K, pH 7.2 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | maltodextrin-binding protein | [U-2H; U-15N; U-13C] | 1.3 mM | |
2 | maltotriose | 1.3 mM |