BMRB: 5331

Backbone relaxation data of rat holo cellular retinol-binding protein type I (CRBP-I)

Authors

Franzoni, L., Luecke, C., Perez, C., Cavazzini, D., Rademacher, M., Ludwig, C., Spisni, A., Rossi, G., Rueterjans, H.

Assembly

cellular retinol-binding protein type I

Entity

1. cellular retinol-binding protein type I (polymer, Thiol state: all free), 135 monomers, 15833.88 Da Detail

MPVDFNGYWK MLSNENFEEY LRALDVNVAL RKIANLLKPD KEIVQDGDHM IIRTLSTFRN YIMDFQVGKE FEEDLTGIDD RKCMTTVSWD GDKLQCVQKG EKEGRGWTQW IEGDELHLEM RAEGVTCKQV FKKVH

2. RTL (non-polymer), 286.452 Da

Total weight

16120.332 Da

Max. entity weight

15833.88 Da

Source organism

Rattus norvegicus

Exptl. method

NMR

Refine. method

TORSION ANGLE DYNAMICS COMBINED WITH SIMULATED ANNEALING FOLLOWED BY ENERGY MINIMIZATION

Data set

order_parameters, heteronucl_T1_relaxation, heteronucl_T2_relaxation, heteronucl_NOEs

Protein Blocks Logo

Calculated from 20 models in PDB: 1JBH, Strand ID: A Detail

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Heteronucl. T₁

235 T₁ values in 2 lists
Coherence Sz, Field strength (¹H) 500 MHz, 600 MHz, Temperature 298 (±0.1) K, pH 6.0 (±0.1) Detail

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Temperature 298 (±0.1) K, pH 6.0 (±0.1)

Heteronucl. T₂

236 T₂ values in 2 lists
Coherence S(+,-), Field strength (¹H) 500 MHz, 600 MHz, Temperature 298 (±0.1) K, pH 6.0 (±0.1) Detail

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Temperature 298 (±0.1) K, pH 6.0 (±0.1)

Heteronucl. NOE

234 NOE values in 2 lists
Value type relative intensities, Field strength (¹H) 500 MHz, 600 MHz, Temperature 298 (±0.1) K, pH 6.0 (±0.1) Detail

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Temperature 298 (±0.1) K, pH 6.0 (±0.1)

Heteronucl. T₁/T₂

235 T₁/T₂ values in 2 lists
Field strength (¹H) 500 MHz, 600 MHz, Temperature 298 (±0.1) K, pH 6.0 (±0.1) Detail

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Temperature 298 (±0.1) K, pH 6.0 (±0.1)

Order parameters

118 S² values in 1 lists
Temperature 298 (±0.1) K, pH 6.0 (±0.1) Detail

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Temperature 298 (±0.1) K, pH 6.0 (±0.1)

List #1 S2

Release date

2002-06-12

Citation

Structure and backbone dynamics of Apo- and holo-cellular retinol-binding protein in solution
Franzoni, L., Luecke, C., Perez, C., Cavazzini, D., Rademacher, M., Ludwig, C., Spisni, A., Rossi, G., Rueterjans, H.
J. Biol. Chem. (2002), 277, 21983-21997, PubMed 11934897 , DOI 10.1074/jbc.M201994200 , Abstract

Related entities 1. cellular retinol-binding protein type I, : 1 : 3 : 27 : 214 entities Detail

Interaction partners 1. cellular retinol-binding protein type I, : 2 interactors Detail

Experiments performed 3 experiments Detail