BMRBj - BMREntryMaster

Found 1 Document (1.589 seconds)

BMRB: 7415

2JXY

Evidence of reciprocical reorientation of the catalytic and hemopexin-like domains of full-length MMP-12

Authors: Bertini, I., Calderone, V., Fragai, M., Jaiswal, R., Luchinat, C., Melikian, M., Mylonas, E., Svergun, D.I.
Assembly: MMP12 HUMAN
Entity: 1. CAT DOMAIN (polymer, Thiol state: not present), 159 monomers, 17624.55 Da Detail
MGPVWRKHYI TYRINNYTPD MNREDVDYAI RKAFQVWSNV TPLKFSKINT GMADILVVFA RGAHGDFHAF DGKGGILAHA FGPGSGIGGD AHFDEDEFWT THSGGTNLFL TAVHEIGHSL GLGHSSDPKA VMFPTYKYVD INTFRLSADD IRGIQSLYG

2. CD (CADMIUM ION) (non-polymer), 1 monomers, 112.411 Da
Total weight: 17736.96 Da
Max. entity weight: 17624.55 Da
Source organism: Homo sapiens
Exptl. method: NMR
Data set: heteronucl_NOEs, heteronucl_T1_relaxation, heteronucl_T2_relaxation
Heteronucl. T₁: 129 T₁ values in 1 lists
Coherence Sz, Field strength (¹H) 700 MHz, Pressure 1 atm, Temperature 298 K, pH 7.2 Detail
Pressure 1 atm, Temperature 298 K, pH 7.2
Heteronucl. T₂: 129 T₂ values in 1 lists
Coherence S(+,-), Field strength (¹H) 700 MHz, Pressure 1 atm, Temperature 298 K, pH 7.2 Detail
Pressure 1 atm, Temperature 298 K, pH 7.2
Heteronucl. NOE: 126 NOE values in 1 lists
Value type peak integral, Field strength (¹H) 700 MHz, Pressure 1 atm, Temperature 298 K, pH 7.2 Detail
Pressure 1 atm, Temperature 298 K, pH 7.2
Heteronucl. T₁/T₂: 129 T₁/T₂ values in 1 lists
Field strength (¹H) 700 MHz, Pressure 1 atm, Temperature 298 K, pH 7.2 Detail
Pressure 1 atm, Temperature 298 K, pH 7.2
Release date: 2011-08-10
Citation: Evidence of reciprocal reorientation of the catalytic and hemopexin-like domains of full-length MMP-12
Bertini, I., Calderone, V., Fragai, M., Jaiswal, R., Luchinat, C., Melikian, M., Mylonas, E., Svergun, D.I.
J. Am. Chem. Soc. (2008), 130, 7011-7021, PubMed 18465858 , DOI 10.1021/ja710491y , Abstract

Related entities 1. CAT DOMAIN, : 3 : 80 : 196 entities Detail

Interaction partners 1. CAT DOMAIN, : 1 interactors Detail

More details for 1 interactors identified by 1 citations

Experiments performed 15 experiments Detail

1 3D_15N-separated_NOESY

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

2 3D_13C-separated_NOESY

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

3 2D 1H-15N HSQC

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

4 3D HNCO

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

5 3D HNCA

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

6 3D HN(CO)CA

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

7 3D CBCA(CO)NH

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

8 3D HNCACB

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

9 3D HCCH-TOCSY

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

10 3D HBHA(CO)NH

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

11 3D HNHA

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

12 2D 1H-15N HSQC T1

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

13 2D 1H-15N HSQC T2

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

14 2D 1H-15N HSQC NOE

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

15 2D 1H-15N HSQC IPAP

Instrument

Bruker AVANCE - 900 MHz TCI probe

Sample

State isotropic, Pressure 1 atm, Temperature 298 K, pH 7.2, Details pH 6.5, no buffer

#	Name	Isotope labeling	Type	Concentration
1	CAT_DOMAIN	[U-13C; U-15N]		0.0 ~ 0.0 mM
2	NaCl			300 mM

nullKeywords assignment, matrix metalloproteinase, mobility, NMR, RDC

Search

Query history

Resources

Search for primary databases

Search for subsidiary databases

Display

Hits per page

Statistics

Query Changes will take effect after "OK" button is selected.

Maximum hits

Default conjunction operator

Omni-box

Search filter

Sequence search (BLAST)

E-value

Query sequence coverage

Miscellaneous

The number of previewed publications

Completeness of assigned chemical shift

Sequence chart about top aligned regions

Sequence chart about interacting regions

Hit context with highlight

Link destinations for BMRB, PDB and EMDB

Found 1 Document (1.589 seconds)

BMRB: 7415

Related entities 1. CAT DOMAIN, : 3 : 80 : 196 entities Detail

Interaction partners 1. CAT DOMAIN, : 1 interactors Detail

Experiments performed 15 experiments Detail

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample

Instrument

Sample