Backbone H, CA, N Chemical Shift Assignments for C2A/Ca2+ Binary Complex
EKLGKLQYSL DYDFQNNQLL VGIIQAAELP ALDMGGTSDP YVKVFLLPEK KKKFETKVHR KTLNPVFNEQ FTFKVPYSEL GGKTLVMAVY DFDRFSKHDI IGEFKVPMNT VDFGHVTEEW RDLQSAEK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 24.3 % (383 of 1576) | 15.9 % (131 of 823) | 22.0 % (136 of 619) | 86.6 % (116 of 134) |
Backbone | 49.1 % (371 of 756) | 46.9 % (121 of 258) | 35.6 % (134 of 376) | 95.1 % (116 of 122) |
Sidechain | 1.9 % (18 of 940) | 1.8 % (10 of 565) | 2.2 % (8 of 363) | 0.0 % (0 of 12) |
Aromatic | 1.2 % (2 of 164) | 2.4 % (2 of 82) | 0.0 % (0 of 81) | 0.0 % (0 of 1) |
Methyl | 2.9 % (4 of 136) | 2.9 % (2 of 68) | 2.9 % (2 of 68) |
1. C2A domain of synaptotagmin I
EKLGKLQYSL DYDFQNNQLL VGIIQAAELP ALDMGGTSDP YVKVFLLPEK KKKFETKVHR KTLNPVFNEQ FTFKVPYSEL GGKTLVMAVY DFDRFSKHDI IGEFKVPMNT VDFGHVTEEW RDLQSAEKTemperature 303 (±1) K, pH 7.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | C2A domain of synaptotagmin I | [U-99% 13C; U-99% 15N] | 1.0 mM |