Backbone H, CA, N chemical shift assignments for C2A/Ca2+/6PS ternary complex
EKLGKLQYSL DYDFQNNQLL VGIIQAAELP ALDMGGTSDP YVKVFLLPEK KKKFETKVHR KTLNPVFNEQ FTFKVPYSEL GGKTLVMAVY DFDRFSKHDI IGEFKVPMNT VDFGHVTEEW RDLQSAEK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 28.4 % (447 of 1576) | 20.2 % (166 of 823) | 25.8 % (160 of 619) | 90.3 % (121 of 134) |
Backbone | 53.7 % (406 of 756) | 52.3 % (135 of 258) | 39.9 % (150 of 376) | 99.2 % (121 of 122) |
Sidechain | 5.4 % (51 of 940) | 5.5 % (31 of 565) | 5.5 % (20 of 363) | 0.0 % (0 of 12) |
Aromatic | 2.4 % (4 of 164) | 4.9 % (4 of 82) | 0.0 % (0 of 81) | 0.0 % (0 of 1) |
Methyl | 10.3 % (14 of 136) | 11.8 % (8 of 68) | 8.8 % (6 of 68) |
1. C2A domain of synaptotagmin I
EKLGKLQYSL DYDFQNNQLL VGIIQAAELP ALDMGGTSDP YVKVFLLPEK KKKFETKVHR KTLNPVFNEQ FTFKVPYSEL GGKTLVMAVY DFDRFSKHDI IGEFKVPMNT VDFGHVTEEW RDLQSAEKTemperature 303 (±1) K, pH 7.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | C2A domain of synaptotagmin I | [U-99% 13C; U-99% 15N] | 1.0 mM | |
2 | Calcium | 5 mM | ||
3 | na | 5 mM | ||
4 | Tris-HCl | 50 mM | ||
5 | NaCl | 200 mM | ||
6 | DSS | 2 mM |