Backbone 1H, 13C, and 15N Chemical Shift Assignments for the Inhibitor-Bound DNase Domain of Colicin E9.
MESKRNKPGK ATGKGKPVGD KWLDDAGKDS GAPIPDRIAD KLRDKEFKSF DDFRKAVWEE VSKDPELSKN LNPSNKSSVS KGYSPFTPKN QQVGGRKVYE LHHDKPISQG GEVYDMDNIR VTTPKRHIDI HRGK
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 35.5 % (908 of 2556) | 31.0 % (418 of 1348) | 37.2 % (366 of 983) | 55.1 % (124 of 225) |
Backbone | 56.6 % (733 of 1294) | 57.5 % (256 of 445) | 55.1 % (354 of 642) | 59.4 % (123 of 207) |
Sidechain | 18.9 % (276 of 1464) | 18.2 % (164 of 903) | 20.4 % (111 of 543) | 5.6 % (1 of 18) |
Aromatic | 1.6 % (3 of 182) | 2.2 % (2 of 91) | 1.1 % (1 of 88) | 0.0 % (0 of 3) |
Methyl | 9.7 % (17 of 176) | 11.4 % (10 of 88) | 8.0 % (7 of 88) |
1. DNase domain of colicin E9
MESKRNKPGK ATGKGKPVGD KWLDDAGKDS GAPIPDRIAD KLRDKEFKSF DDFRKAVWEE VSKDPELSKN LNPSNKSSVS KGYSPFTPKN QQVGGRKVYE LHHDKPISQG GEVYDMDNIR VTTPKRHIDI HRGK2. Immunity protein of colicin E9
MELKHSISDY TEAEFLQLVT TICNADTSSE EELVKLVTHF EEMTEHPSGS DLIYYPKEGD DDSPSGIVNT VKQWRAANGK SGFKQGTemperature 298 (±1) K, pH 6.2 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNase domain of colicin E9 | [U-99% 13C; U-99% 15N] | 2.0 mM | |
2 | Immunity protein of colicin E9 | 2.5 mM | ||
3 | Potassium_phosphate | 50.0 mM | ||
4 | H20 | 90 % | ||
5 | D20 | 10 % | ||
6 | Sodium_azide | 0.01 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 25.2 % (1287 of 5112) | 22.4 % (603 of 2696) | 26.1 % (513 of 1966) | 38.0 % (171 of 450) |
Backbone | 38.6 % (1000 of 2588) | 39.4 % (351 of 890) | 37.3 % (479 of 1284) | 41.1 % (170 of 414) |
Sidechain | 14.5 % (424 of 2928) | 14.1 % (254 of 1806) | 15.6 % (169 of 1086) | 2.8 % (1 of 36) |
Aromatic | 0.8 % (3 of 364) | 1.1 % (2 of 182) | 0.6 % (1 of 176) | 0.0 % (0 of 6) |
Methyl | 7.4 % (26 of 352) | 9.1 % (16 of 176) | 5.7 % (10 of 176) |
1. DNase domain of colicin E9
MESKRNKPGK ATGKGKPVGD KWLDDAGKDS GAPIPDRIAD KLRDKEFKSF DDFRKAVWEE VSKDPELSKN LNPSNKSSVS KGYSPFTPKN QQVGGRKVYE LHHDKPISQG GEVYDMDNIR VTTPKRHIDI HRGK2. Immunity protein of colicin E9
MELKHSISDY TEAEFLQLVT TICNADTSSE EELVKLVTHF EEMTEHPSGS DLIYYPKEGD DDSPSGIVNT VKQWRAANGK SGFKQGTemperature 298 (±1) K, pH 6.2 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNase domain of colicin E9 | [U-99% 13C; U-99% 15N] | 2.0 mM | |
2 | Immunity protein of colicin E9 | 2.5 mM | ||
3 | Potassium_phosphate | 50.0 mM | ||
4 | H20 | 90 % | ||
5 | D20 | 10 % | ||
6 | Sodium_azide | 0.01 % |