1H, 13C, and 15N Chemical Shift Assignments for the N-terminal receiver domain of NtrC (unphosphorylated)
MQRGIVWVVD DDSSIRWVLE RALAGAGLTC TTFENGNEVL AALASKTPDV LLSDIRMPGM DGLALLKQIK QRHPMLPVII MTAHSDLDAA VSAYQQGAFD YLPKPFDIDE AVALVERAIS HYQE
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 83.7 % (1177 of 1407) | 91.8 % (663 of 722) | 72.5 % (404 of 557) | 85.9 % (110 of 128) |
Backbone | 79.0 % (578 of 732) | 93.6 % (233 of 249) | 66.0 % (241 of 365) | 88.1 % (104 of 118) |
Sidechain | 89.3 % (707 of 792) | 90.9 % (430 of 473) | 87.7 % (271 of 309) | 60.0 % (6 of 10) |
Aromatic | 82.2 % (74 of 90) | 95.6 % (43 of 45) | 67.4 % (29 of 43) | 100.0 % (2 of 2) |
Methyl | 97.0 % (163 of 168) | 97.6 % (82 of 84) | 96.4 % (81 of 84) |
1. Nitrogen regulatory protein C N-terminal receiver domain
MQRGIVWVVD DDSSIRWVLE RALAGAGLTC TTFENGNEVL AALASKTPDV LLSDIRMPGM DGLALLKQIK QRHPMLPVII MTAHSDLDAA VSAYQQGAFD YLPKPFDIDE AVALVERAIS HYQEPressure 1 atm, Temperature 298 (±1) K, pH 6.75 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Nitrogen regulatory protein C N-terminal receiver domain | [U-15N] | 1 mM | |
2 | sodium phosphate | 50 mM |