Backbone and side-chain 1H, 13C, and 15N chemical shift assignments for chick cofilin
MASGVTVNDE VIKVFNDMKV RKSSTPEEIK KRKKAVLFCL SDDKKQIIVE EAKQILVGDI GDTVEDPYTA FVKLLPLNDC RYALYDATYE TKESKKEDLV FIFWAPESAP LKSKMIYASS KDAIKKKFTG IKHEWQVNGL DDIKDRSTLG EKLGGNVVVS LEGKPL
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 94.3 % (1873 of 1986) | 97.8 % (1015 of 1038) | 89.6 % (697 of 778) | 94.7 % (161 of 170) |
Backbone | 96.2 % (947 of 984) | 96.7 % (324 of 335) | 96.5 % (472 of 489) | 94.4 % (151 of 160) |
Sidechain | 93.2 % (1080 of 1159) | 98.3 % (691 of 703) | 85.0 % (379 of 446) | 100.0 % (10 of 10) |
Aromatic | 53.1 % (68 of 128) | 100.0 % (64 of 64) | 3.2 % (2 of 62) | 100.0 % (2 of 2) |
Methyl | 99.5 % (195 of 196) | 99.0 % (97 of 98) | 100.0 % (98 of 98) |
1. chick cofilin
MASGVTVNDE VIKVFNDMKV RKSSTPEEIK KRKKAVLFCL SDDKKQIIVE EAKQILVGDI GDTVEDPYTA FVKLLPLNDC RYALYDATYE TKESKKEDLV FIFWAPESAP LKSKMIYASS KDAIKKKFTG IKHEWQVNGL DDIKDRSTLG EKLGGNVVVS LEGKPLTemperature 298 (±0.5) K, pH 6.8 (±0.05)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | chick cofilin | [U-99% 15N] | 1.0 mM | |
2 | NaCl | 50 mM | ||
3 | PIPES | 10 mM | ||
4 | H2O | 92.5 % | ||
5 | D2O | 7.5 % |
Temperature 298 (±0.5) K, pH 6.8 (±0.05)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | chick cofilin | [U-99% 13C; U-99% 15N] | 1.0 mM | |
7 | NaCl | 50 mM | ||
8 | PIPES | 10 mM | ||
9 | H2O | 92.5 % | ||
10 | D2O | 7.5 % |
Temperature 298 (±0.5) K, pH 6.8 (±0.05)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
11 | chick cofilin | [U-99% 13C; U-99% 15N] | 1.0 mM | |
12 | NaCl | 50 mM | ||
13 | PIPES | 10 mM | ||
14 | D2O | 100 % |