Backbone 15N and 1HN Chemical Shift Assignments for Sac7d
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 18.0 % (145 of 807) | 18.1 % (78 of 430) | 0.3 % (1 of 310) | 98.5 % (66 of 67) |
Backbone | 33.5 % (132 of 394) | 49.3 % (67 of 136) | 0.5 % (1 of 193) | 98.5 % (64 of 65) |
Sidechain | 2.7 % (13 of 474) | 3.7 % (11 of 294) | 0.0 % (0 of 178) | 100.0 % (2 of 2) |
Aromatic | 4.2 % (2 of 48) | 4.2 % (1 of 24) | 0.0 % (0 of 23) | 100.0 % (1 of 1) |
Methyl | 0.0 % (0 of 58) | 0.0 % (0 of 29) | 0.0 % (0 of 29) |
1. Sac7d
MVKVKFKYKG EEKEVDTSKI KKVWRVGKMV SFTYDDNGKT GRGAVSEKDA PKELLDMLAR AEREKKTemperature 303 (±1) K, pH 4.07 (±0.1)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Sac7d | [U-98% 15N] | 1.2 mM | |
2 | KCl | 0.3 M | ||
3 | H2O | 90 % | ||
4 | D2O | 10 % | ||
5 | DSS | 100 uM |