BMRB: 6413

FRAGMENT 33-61 OF BOVINE alpha-HEMOGLBIN: THE EFFECT OF C-TERMINAL AMIDATION AND IDENTIFICATION OF THE MINIMAL PORTION WITH ANTIFUNGAL ACTIVITY

Authors

Machado, A., Sforca, M.L., Miranda, A., Daffre, S., Spisni, A., Pertinhez, T.A., Miranda, M.M.

Assembly

fragment 40-61

Entity

1. fragment 40-61 (polymer, Thiol state: not present), 22 monomers, 2412.657 Da Detail

KTYFPHFDLS HGSAQVKGHG AK

Formula weight

2412.657 Da

Source organism

Bos taurus

Exptl. method

NMR

Data set

assigned_chemical_shifts, coupling_constants

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 76.5 %, Completeness (bb): 91.3 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	76.5 % (101 of 132)	76.5 % (101 of 132)
Backbone	91.3 % (42 of 46)	91.3 % (42 of 46)
Sidechain	68.6 % (59 of 86)	68.6 % (59 of 86)
Aromatic	60.0 % (12 of 20)	60.0 % (12 of 20)
Methyl	71.4 % (5 of 7)	71.4 % (5 of 7)

1. fragment 40-61

KTYFPHFDLS HGSAQVKGHG AK

Show sample condition

Sample

Temperature 310 (±1) K, pH 4.0 (±0.2)

#	Name	Isotope labeling	Type	Concentration
1	fragment 40-61			1.0 mM
2	sodium dodecyl sulfate (SDS)			200 mM

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Coupling constant

17 J values in 1 lists
Temperature 310 (±1) K, pH 4.0 (±0.2) Detail

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Temperature 310 (±1) K, pH 4.0 (±0.2)

List #1 J_values_set_1

Release date

2005-10-19

Citation 1

The micelle-bound structure of an antimicrobial peptide derived from the alpha-chain of bovine hemoglobin isolated from the tick Boophilus microplus
Sforca, M.L., Machado, A., Figueredo, R.C., Oyama, S., Silva, F.D., Miranda, A., Daffre, S., Miranda, M.TERESA., Spisni, A., Pertinhez, T.A.
Biochemistry (2005), 44, 6440-6451, PubMed 15850378 , DOI 10.1021/bi0475323 , Abstract

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Citation 2

NMRPipe: a multidimensional spectral processing system based on UNIX pipes
Delaglio, F., Grzesiek, S., Vuister, G.W., Zhu, G., Pfeifer, J., Bax, A.
J. Biomol. NMR (1995), 6, 277-293, PubMed 8520220 , Abstract

Hide non-primary 1 citaion

Related entities 1. fragment 40-61, : 1 : 20 : 1 : 155 : 43 entities Detail

Interaction partners 1. fragment 40-61, : 32 interactors Detail

Experiments performed 4 experiments Detail

Chemical shift validation 3 contents Detail