NMR chemical shift entry for protein Rv1980c (MPT64) from M. tuberculosis
MAPKTYCEEL KGTDTGQACQ IQMSDPAYNI NISLPSYYPD QKSLENYIAQ TRDKFLSAAT SSTPREAPYE LNITSATYQS AIPPRGTQAV VLKVYQNAGG THPTTTYKAF DWDQAYRKPI TYDTLWQADT DPLPVVFPIV QGELSKQTGQ QVSIAPNAGL DPVNYQNFAV TNDGVIFFFN PGELLPEAAG PTQVLVPRSA IDSMLA
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS7:SG | 1:CYS19:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 87.6 % (2060 of 2352) | 83.9 % (1019 of 1215) | 91.3 % (842 of 922) | 92.6 % (199 of 215) |
Backbone | 96.9 % (1161 of 1198) | 95.8 % (387 of 404) | 97.7 % (593 of 607) | 96.8 % (181 of 187) |
Sidechain | 80.8 % (1090 of 1349) | 77.9 % (632 of 811) | 86.3 % (440 of 510) | 64.3 % (18 of 28) |
Aromatic | 55.7 % (108 of 194) | 54.6 % (53 of 97) | 57.9 % (55 of 95) | 0.0 % (0 of 2) |
Methyl | 95.2 % (217 of 228) | 94.7 % (108 of 114) | 95.6 % (109 of 114) |
1. Rv1980c (MPT64) polypeptide
MAPKTYCEEL KGTDTGQACQ IQMSDPAYNI NISLPSYYPD QKSLENYIAQ TRDKFLSAAT SSTPREAPYE LNITSATYQS AIPPRGTQAV VLKVYQNAGG THPTTTYKAF DWDQAYRKPI TYDTLWQADT DPLPVVFPIV QGELSKQTGQ QVSIAPNAGL DPVNYQNFAV TNDGVIFFFN PGELLPEAAG PTQVLVPRSA IDSMLATemperature 303 (±0.1) K, pH 6.85 (±0.03), Details MES, D2O, NaN3, DSS
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Rv1980c (MPT64) polypeptide | [U-15N; U-13C] | protein | 2.0 (±0.05) mM |
2 | MES | buffer | 20 mM | |
3 | D2O | 5 % | ||
4 | NaN3 | 1 mM | ||
5 | DSS | internal reference | 0.2 mM |